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This paper has reported the beneficiation and characterization of gold from Itagunmodi gold ore in Atakumosa West LGA in the State of Osun Nigeria using cyanide solution obtained from cassava and commercially available sodium cyanide analar grade. Cyanide solution extracted from cassava variety TMS 30572 leaves obtained from Obafemi Awolowo University (O.A.U) Research and Teaching Farm was discovered to have the highest free cyanide (CN − ) among the ten different cassava varieties evaluated.doi:10.4236/jmmce.2014.24035 fatcat:n42xfri3qrfobd2x3yxpvxwapm