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Zirconia particles were prepared by thermal treatment of zirconium(IV) tetra-n-propoxide (ZNP) in C 2 C 6 glycols (Glycothermal method) at 300°C and morphology and pore structures of the products were examined. Xray diffraction results revealed that nanocrystals of tetragonal zirconia phase were mainly obtained in all cases. However, the morphology and pore structures of the products were quite different depending on the glycols used. The products prepared in 1,4-butanediol (1,4-BG) weredoi:10.2109/jcersj2.20011 fatcat:llhoxgaybnhozn5kxyhrg3wiem