Access to functionalised silver(i) and gold(i) N-heterocyclic carbenes by [2 + 3] dipolar cycloadditions

Audrey Hospital, Clémentine Gibard, Christelle Gaulier, Lionel Nauton, Vincent Théry, Malika El-Ghozzi, Daniel Avignant, Federico Cisnetti, Arnaud Gautier
2012 Dalton Transactions  
Supporting information Contents: S1: Crystal packing of 22 S2: Selected NMR spectra. e 3.08 (ddd, 2H, 3 J = 3.0 Hz, 3 J = 7.5 Hz, 2 J =16.0 Hz), 2.99-2.90 (m, 4H), 2.78 (ddd, 2H, 3 J = 3.0 Hz, 3 J = 9.5 Hz, 2 J =16.0 Hz) 26.5, 24.5 f 7.65 (s, 4H) 124.0 g 2.61 (hept, 4H, 3 J = 7.0 Hz) 31.0 h 1.41 (d, 3 J = 7.0 Hz ), 1.33 (d, 3 J = 7.0 Hz) 24.74, 24.72, 23.7-23.8 (2 signals)* i 8.50 (d, 2H, 4 J = 1.5 Hz) 128.1 j 10.24 (t, 1H, 4 J = 1.5 Hz) 141.2 Electronic Supplementary Material (ESI) for Dalton
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doi:10.1039/c2dt30249g pmid:22517562 fatcat:3hmlotgqgbh4nl2xjocftr7xgy