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A new approach has been used to prepare nanostructured lead oxide-carbon ͑PbO-C͒ composites via the spray pyrolysis technique. In this study, the electrochemical performance of the PbO-carbon nanocomposites as anode materials for lithium-ion rechargeable batteries was investigated. The prepared powders consist of fine nanocrystalline PbO homogeneously distributed within an amorphous carbon matrix with highly developed surface area. The estimated average crystal sizes of these nanocompositesdoi:10.1149/1.2172570 fatcat:nv24subc5rbnhadc4lv2xnz3da