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The use of a microcalorimeter X-ray detector with a transition edge sensor in an electron probe to perform quantitative analysis is reported. Two bulk samples of multielement glasses that have been previously characterized by chemical methods for use as standard reference materials were analyzed. The spectra were analyzed against standards using three different correction schemes. In one of the standards, the reference line was easily resolved despite its proximity within 45 eV of another line.doi:10.1154/1.2737466 fatcat:xg3aoiup6fblbdldnsyeequuma