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Hollow cathode lamp excited inductively coupled plasma atomic fluorescence spectrometry for metal determination in organic solvents

K. S. YEAH, W. MASAMBA, J. D. WINEFORDNER
1987 Analytical Sciences  

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The hollow cathode lamp-inductively coupled plasma-atomic fluorescence spectrometer system (Baird) has been evaluated for the measurement of Na, Cu, Ni, Ag, Fe, AI, Cr and Mg in a variety of organic solvents. Kerosene proved to be the best solvent. The system was evaluated for the effect of solution flow rate, oil content, 02 flow rate, RF power and observation height for the measurement of those eight elements in a 2% oil-98% kerosene mixture. Analytical figures of merit, including detection
more » ... mits, linear ranges of response, stability with time, and spectral interferences, were evaluated for the 8 elements present as metallorganic compounds. The analysis of several standard reference materials showed excellent agreement with the certified values.
doi:10.2116/analsci.3.245 fatcat:rmads7j7nnfwfdkvlqasekovgy
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K. S. YEAH, W. MASAMBA, J. D. WINEFORDNER. "Hollow cathode lamp excited inductively coupled plasma atomic fluorescence spectrometry for metal determination in organic solvents." Analytical Sciences 3.3 (1987) 245-249