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We report that ethanol, used together with water, plays a crucial role in tuning the structures of a zirconium-based metal–organic framework and the 12-connected MOF-801, as well as the possible mechanisms of this modulating effect. By employing a cosolvent system of ethanol and water at just under room temperature without the presence of a monotopic carboxylic acid as the modulator, MOF-801 in various morphologies of different sizes could be synthesized. A linear correlation between thedoi:10.3390/cryst11040434 fatcat:xczanofkjjgwdi3g7vv7fn5g6m