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Recebido em 27/3/12; aceito em 20/10/12; publicado na web em 21/2/13 A simple, sensitive and selective cloud point extraction procedure is described for the preconcentration and atomic absorption spectrometric determination of Zn 2+ and Cd 2+ ions in water and biological samples, after complexation with 3,3',3",3'"-tetraindolyl (terephthaloyl) dimethane (TTDM) in basic medium, using Triton X-114 as nonionic surfactant. Detection limits of 3.0 and 2.0 μg L -1 and quantification limits 10.0 anddoi:10.1590/s0100-40422013000300004 fatcat:tdrox5ndnndmhocxaupsp5s7uq