Internet Archive Scholar

X-RAY ANALYSIS FOR DETERMINATION THE CRYSTALLITE SIZE AND LATTICE STRAIN IN ZnO NANOPARTICLES

H Wasly
2018 Journal of Al-Azhar University Engineering Sector  

Preserved Fulltext

fulltext thumbnail
Web Archive Capture PDF (992.8 kB)
https://web.archive.org/web/20190429050028/https://jaes.journals.ekb.eg/article_18943_870b957c1f5690bdc650d1bb8f0bc416.pdf

A copy of this work was available on the public web and has been preserved in the Wayback Machine. The capture dates from 2019; you can also visit the original URL. The file type is application/pdf.

Zinc oxide (ZnO) nanoparticles were synthesized by modified hydrothermal method at 160 o C under different reaction times. The analysis of the XRD pattern lines is considered a simple and effective method in estimating the crystallite size and the corresponding lattice strain. Xray patterns were analyzed using Scherrer method and Williamson-Hall treatment to determine the crystallite size and the lattice strain. The XRD pattern confirmed the presence of crystalline hexagonal wurtzite ZnO
more » ... ticles with average crystallite size in the range 30 -36 nm with different reaction times. ZnO nanoparticles were also characterized by high resolution transmission electron microscopy (HR-TEM), UV-visible spectroscopy and thermal analysis.
doi:10.21608/auej.2018.18943 fatcat:qruvab4vobe4hj44jqp5odayh4
Citation

H Wasly. "X-RAY ANALYSIS FOR DETERMINATION THE CRYSTALLITE SIZE AND LATTICE STRAIN IN ZnO NANOPARTICLES." Journal of Al-Azhar University Engineering Sector 13.49 (2018) 1312-1320