Crystal structure of 4,5,9,10-tetrathiocino[1,2-b;5,6-b']diimidazolyl- 1,3,6,8-tetraphenyl-2,7-dithione — dichloromethane (1:1), C30H20N4S6 · CH2Cl2

Agnes Bittermann, Benno Bildstein, Klaus Wurst
2008 Zeitschrift für Kristallographie - New Crystal Structures  
C 31H22Cl2N4S6, monoclinic, C12/c1 (no. 15), a = 21.9970(5) Å, b = 13.6104(5) Å, c = 23.1275(9) Å, b = 92.525(2)°, V = 6917.4 Å 3 , Z = 8, Rgt(F) = 0.054, wR ref (F 2 ) = 0.163, T = 233 K. Source of material The title compound was obtained by reaction of 1,3-diphenyl-4,5-imidazolidine-4,5-dione with Lawesson's reagent and nickel chloride in refluxing toluene. Experimental details Hydrogen atoms were calculated and refined using a riding model and were not established for the disordered solvent
more » ... disordered solvent molecules.
doi:10.1524/ncrs.2008.0097 fatcat:hmfhbtqz6rd5dnyd7hklayv6re