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Chemico-thermal synthesis of nano-structured cobalt with distinct magnetic property
unpublished
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The synthesis of nanostructures cobalt through a controlled chemical process followed by heat treating at various temperatures is studied. The product is characterized by ICP, XRD, FESEM, and TEM, indicating that the as-synthesized particles have an amorphous structure with 1.76 for Co/B ratio, an average size of 50 nm. The transformation of intermediate phases into single phase nano-crystalline metallic cobalt during the heat treatment is investigated by DSC analysis. The mean crystallite size
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