A novel series of 5-{(4-amino-N-[2-(diethylamino)ethyl]-o-anisamido-5-yl}-amino-3-substitutedimino-7- substitutedimino-1,2,4,6-trithiazepines was synthesized by the interactions of 4-amino-5-substituteddithiobiureto-N- [2-(diethylamino)ethyl]-o-anisamides with phenylisothio carbamoyldichloride in acetone-ethanol medium. The structures of all the synthesized compounds were justified on the basis of chemical characteristics, elemental analysis and spectral studies. Keywords:

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... hylamino)ethyl]-o-anisamido-5-yl}-amino-3-phenylimino-7-ethylimino-1,2,4,6- trithiazepine, 4-amino-5-phenyldithiobiureto-N-[2-(diethylamino) ethyl]-o-anisamide, phenylisothiocarbamoylchloride, acetone-ethanol medium.