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Anwendung der 11B-NMR-Spektroskopie zur Untersuchung von Hydroborierungen, II [1]Hydroborierung von 1.5-Cyclooctadien mit Boran in Tetrahydrofuran / Application of 11B NMR Spectroscopy to the Study of Hydroboration, II [1] Hydroboration of 1,5-Cyclooctadiene with Borane in Tetrahydrofurane
1980
Zeitschrift für Naturforschung. B, A journal of chemical sciences
Preserved Fulltext
The existence of various intermediates in the hydroboration of 1,5-cyclooctadiene with borane in tetrahydrofurane (BH3-THF) is revealed by 11B NMR spectroscopy. The presence of the THF adduct of 9-borabicyclo[3,3,1]nonane in solutions of the dimer in THF is proved for the first time, and the importance of the adduct in accelerating exchange reactions shown by 11B NMR spectroscopy.
doi:10.1515/znb-1980-1012
fatcat:7yvpnyexfjauxowlzes5wp6fda