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Vermiculite-based nano-adsorbent was successfully prepared via solution casting method from vermiculite that was first exfoliated by thermal shock followed by ultrasonic treatment. X-ray diffraction investigations showed that the combined effect of sonication and organo-modification led to extensive delamination of the vermiculite sheets. BET surface area measurements indicated flake thicknesses below 100 nm. Scanning electron microscopy images revealed that the organo-modification process ofdoi:10.3303/cet2081180 doaj:c2c96d4fae714dd290bce663ffd5273b fatcat:zrxszixllrdtlf4hi5iic7tcki