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Three-dimensional microstructure of a conventional Ni-8YSZ anode is quantified by means of dual beam FIB-SEM system equipped with EDX. The microstructure of the anode is virtually reconstructed in a computational field using a series of twodimensional SEM images acquired. Three-phase-boundary (TPB) density and tortuosity factors are carefully evaluated applying two different evaluation methods to each parameter. TPB density is evaluated by volume expansion method and centroid method, whiledoi:10.1149/1.3205723 fatcat:pp2hljd7evb5hnrghmxiz5vasa