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Crystal structure of N,N-diethyl-5-bromo-3,4-dihydro-2,4-dioxopyrimidine-1(2H)-carboxamide, C9H12BrN3O3
2017
Zeitschrift für Kristallographie - New Crystal Structures
Preserved Fulltext
C 9 H 12 BrN 3 O 3 , monoclinic, P21/c, a = 12.0359(15) Å, b = 5.4815(6) Å, c = 20.1931(18) Å, β = 120.780(5)°, V = 1144.6(2) Å 3 , Z = 4, Rgt(F) = 0.0234, wR ref (F 2 ) = 0.0984, T = 298(2) K. CCDC no.: 849470 The crystal structure is shown in the gure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters. Source of material 5-Bromouracil (0.29 g, 1 mmol), bis(trichloromethyl) carbonate (0.118 g, 0.4 mmol), anhydrous dichloromethane (DCM)
doi:10.1515/ncrs-2016-0169
fatcat:743t2dolubfjjellwdfuriorda