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A new mixed halo chromate nanoparticle compound was synthesised and characterized. Triphenylphosphonium trifluoroiodochromate (III)[P(C 6 H 5) 3 H] + [CrF 3 I]-nanoparticle was synthesized by using triphenylphosphonium iodide reaction with CrF 3, in the presence of 3-mercaptopropionic acid. This method is a simple and direct method. The product was characterized by spectroscopic and analytical methods such as 31 P-NMR, FT-IR, XRD, SEM. Theoretical calculations were used for the structuralfatcat:73mdkeaefvc47oomg7rapbonfu