SYNTHESIS, SPECTROSCOPIC CHARACTERISATION, AND KINETIC PARAMETER STUDY OF LABILE CHROMIUM COMPLEXES USING BENZOIC ACID AS A LIGAND

M.K. Mishra, R.K. Singh
2022 RASAYAN Journal of Chemistry  
Ethanol was used as the solvent in the process of producing chromium benzoic acid complexes by combining CrO3 (chromium trioxide) and benzoic acid. Its spectrum characteristics were evaluated by the use of elemental analysis, FAB-Mass Spectroscopy,1 HNMR spectroscopy, FTIR Spectroscopy, UV-Vis Spectroscopy, and ICP-OES, and its thermal decomposition has been studied through DSC. The Objective was to get inside of thermal stability, the heat of energy, and the rate of decomposition of the
more » ... es. The kinetic parameter, low amount of activation energy, and enthalpy of reaction, all pointed to the complexes having a high degree of liability.
doi:10.31788/rjc.2022.1548040 fatcat:dwnpruurizaphmfknlrrjnvoau