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Titanium hydride was successfully synthesized at room temperature by ball milling. X-ray diffraction patterns demonstrated that a transformation of elemental Ti powders into TiH 2 could be induced at room temperature by ball milling under a hydrogen atmosphere. Almost no hydrogen absorption was observed during the initial few minutes of the milling process on the basis of x-ray diffraction patterns and hydrogen pressure in the reservoir system, although the grain size of Ti decreaseddoi:10.1088/0022-3727/32/15/323 fatcat:ss66y7duajd6fdklpkbvms6d3m