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Treatment of yellow dye 23 by heterogeneous Fenton-like process was studied using iron rich soil as an iron source. The iron rich soil sample was characterized by XRD, SEM and BET analysis. XRD pattern indicates that the iron rich soil is made of goethite and hematite. The reaction was systematically investigated under various experimental conditions such as pH, iron rich soil dosage, oxidant and dye concentrations. The result revealed that using iron rich soil as catalyst led to highdoi:10.4236/aces.2016.65048 fatcat:cry4nk6ucfcujojrrzbqii5y2q