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Using conventional and high-resolution transmission electron microscopy (HRTEM), the effects of rolling at room temperature on the microstructures of amorphous Al 90 Fe 5 Gd 5 and Al 86.8 Ni 3.7 Y 9.5 were compared. In rolled Al 90 Fe 5 Gd 5 , nanocrystallites were observed at shear bands, whereas none were observed in rolled Al 86.8 Ni 3.7 Y 9.5 . When HRTEM was combined with with Fourier transform filtering, nanoscale, low-density defects were imaged. In Al 90 Fe 5 Gd 5 , the shear bandsdoi:10.1557/jmr.2005.0090 fatcat:eg2snwmrfbh6fam35emf3lgqni