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Synthesis, characterization and magnetic investigation of (NH4)0.5Mn1.25(H2O)2[BP2O8]·0.5H2O
2007
Open Chemistry
AbstractA new borophosphate compound with the composition (NH4)χ Mn((3−χ)/2)(H2O)2 [BP2O8]·(1−x)H2O was prepared under mild hydrothermal conditions and characterized by X-ray powder diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FTIR) methods. The title compound was synthesized from MnCl2·2H2O, H3BO3, and (NH4)2HPO4 with variable molar ratios by heating at 180 °C for 7 days in an autoclave. The X-ray diffraction data of the water insoluble polycrystalline powder was indexed
doi:10.2478/s11532-007-0006-z
fatcat:f3ug2dqpazgynlbcz7dmalxcby