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Crystalline, high surface area, hexagonal mesoporous MCM-41 having uniform pore sizes and good thermal stability was successfully synthesized at 90-120 o C in 30 minutes using low power microwave irradiation. This appears to be the first comprehensive and quantitative investigation of the comparatively rapid synthesis of mesoporous MCM-41 using low power microwave heating of 80W (90 o C) and 120W (120 o C). The influence of reaction temperature and the duration of heating were carefullyfatcat:2haygxhwirfcbi46r2ok4sbgt4