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TiN films consisting of fine crystal grains, with diameters of about 100 nm or less, provided superior hydrogen-permeation barriers. Applying a coating of TiN on a stainless steel substrate reduced the hydrogen permeation by a factor of about 100 to 5,000 compared with uncoated substrates. Effect of microstructure of films on hydrogen-permeation behavior is studied. The test specimens coated with films, with columnar crystals grown vertically on the substrate, tended to exhibit higher hydrogendoi:10.17265/2161-6213/2015.5-6.002 fatcat:tsk2fmhxung47lakadukh3vvcm