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Crystal structure of (1S,2R,4S)-1-((phenylamino)methyl)- 4-(prop-1-en-2-yl)cyclohexane-1,2-diol), C16H23NO2
2011
Zeitschrift für Kristallographie - New Crystal Structures
Source of material Am ixture of aniline (5.1 mmol) and epoxy perillyl alcohol (5 mmol) was added to 0.25 mmol of Ca(CF 3CO2)2 under solvent-free conditions. The mixture was stirred at 40 °Cfor 72 h. After the reaction was finished, the mixture was extracted with AcOEt (3 × 10 mL), dried over Na 2 SO 4 and the solvent was removed at reduced pressure. Colorless crystals of the title compound were isolated by column chromatography on silica gel using hexane/ethyl acetate as eluent (yield 55 %).
doi:10.1524/ncrs.2011.0125
fatcat:6d6wybhn5zejlmgga424nbosqu