Persistence of Imidacloprid and β-Cyfluthrin Residue in Black Pepper (Piper Nigrum L.) Under Malaysia Climatic Condition

Yap Chin Ann, Zehnder Jarroop, A.M.
2016 Journal of Life Sciences  
Persistence behavior of imidacloprid and beta-cyfluthrin in black pepper was studied following application of formulation of Solomon at 0.6 (recommended dose) and 1.2 (double recommended dose) g a.i./ha for one pepper production cycle. The results also showed that the Solomon at 0.6 mL/L concentration significantly suppressed the pest infestation in pepper vines. Pepper vine treated with Solomon produce more berries compared to control and showed no phytotoxicity. Analytical procedure of
more » ... active ingredient was validated prior to actual analysis. Satisfactory recoveries ranging between 87.6%-106.7% were obtained for the fortified pepper berries samples. Results showed low level of imidacloprid and beta-cyfluthrin residues in dried pepper berries ranging between  0.01 mg/kg to 1.43 mg/kg and  0.01 mg/kg to 1.612 mg/kg respectively. The half-life value period for imidacloprid were found to be 2.06 and 2.30 days and for beta-cyfluthrin, these values were observed to be 1.57 and 1.49 days respectively at recommended and double recommended dose. Imidacloprid and beta-cyfluthrin residue dissipated below the limit of quantification (LOQ) of 0.01 mg/kg after 7 and 9 days respectively at recommended and double recommended dose. Soil sample collected 15 days after the last spray did not show the present of Imidacloprid and beta-cyfluthrin residue at their detection limit of 0.01 mg/kg.
doi:10.17265/1934-7391/2016.07.004 fatcat:bu67x3c4mza7lesghml3io7txm