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The reaction of tetramethylsilane with boron tribromide in deuterochloroform in ambient temperature or at 40°C led to bromotrimethylsilane (3) and to dibromomethylborane (4). Identity of products was confirmed by NMR spectroscopy. Analogical reaction carried out in 1,3-dichloropropane allowed to separate products of the reaction and to obtain them in 68% and 59% yields respectively.doi:10.1515/mgmc.2001.24.1.13 fatcat:7xly2fvu3venxgdx34zijkg2de