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Single-crystal Structure and Solid-state NMR of Ga2–xScxO3 (x = 0.83)
2011
Zeitschrift für Naturforschung. B, A journal of chemical sciences
Colorless needles of Ga2−xScxO3 (x = 0.83) were isolated during the crystal growth of La3Ga3Sc2O12 in a K2WO4 flux. The structure was refined from X-ray single-crystal data: β -Ga2O3 type,C2/m, Z = 4, a = 12.716(4), b = 3.1566(6), c = 5.928(5) Å , β = 102.57(3)◦,V = 232.2 Å3, wR2 = 0.0618, 429 F2 values, 32 variables. The structure is based on infinite double chains of edge-sharing Sc/GaO6 octahedra running along the b axis. The GaO4 tetrahedra connect these chains by sharing corners and form a
doi:10.1515/znb-2011-0103
fatcat:bdnsmjrcyzg2lfzo6jtkwoltce