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Titanium metallocarbohedrenes ͑Met-Cars͒ are observed to adsorb methane molecules at low temperatures. The observed formation of the methane-Ti 8 C 12 cluster complexes provides further direct evidence establishing that stable neutral titanium Met-Cars are present in copious amounts in the cluster beam. At sufficiently low temperatures, a dominant peak is observed for Ti 8 C 12 ͑CH 4 ͒ 4 along with less intense peaks of other methane-Ti 8 C 12 clusters, which suggests the geometry of titaniumdoi:10.1063/1.479446 fatcat:okgmhifn7re7znr7ytweqkxfbu