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Three Separate Regions in the Prepared Aniline-Palladium Mixture
2014
American Journal of Physical Chemistry
Polyaniline-palladium composite might be proposed for the electrode material in the oxidation of aliphatic alcohols (methanol, ethanol, ethylene glycol). Prepared mixture of aniline-palladium in sulfuric acid medium (0<рН<1) is investigated by SEM, PXD and FTIR. Obtained results confirm existence of three separate regions: polydisperse palladium powder with agglomerations size of ~0.5 micron in width and ~3-7 microns in length; single palladium particles (~0.5×0.2 micron) coated mainly by
doi:10.11648/j.ajpc.20140301.11
fatcat:mrp6t3cwa5gzrf5rgeskvtglai