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New metal complexes of type M2(HL)2.4H2O[(M = Co(II), Ni (II) and Cu (II)] were prepared using the ligand (HL) =2-[(1H-Pyrrol-2-ylimino methyl)]-5-(2-hydoxy-phenyl)-[1,3,4-thiadiazol]. The Schiff bases were was condensed from [1H-Pyrrole-2-carbaldehyde] with [2-amino-5 -(2-hydroxy-phenyl-1,3,4-thiadiazole] in alcoholic medium. The prepared complexes were characterized by FTIR, UV-vis, 1H-NMR and mass spectra as well as magnetic susceptibility measurements, thermal analysis. The activationdoi:10.22401/jnus.17.3.01 fatcat:wbyizuwhy5gfxios6jp74vvywu