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Two types of new quaternary carbide solid solutions, (ZrC)2Al3[Al1-xGex]C3 (x = 0.07) and (ZrC)3Al3[Al1-yGey]C3 (y = 0.04), have been synthesized and characterized using a laboratory X-ray powder diffractometer (XRPD) and a transmission electron microscope (TEM) equipped with an energy dispersive X-ray analyzer (EDX). With the former carbide, the layered structure was imaged by TEM and the solubility of Ge in the crystal was confirmed by EDX. The crystal structures of both carbides were refineddoi:10.2109/jcersj2.117.22 fatcat:cwg652bv2rgc7cllk3rn4cuhta