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Nanocrystalline powders of ZnO, a-Fe 2 O 3 and ZnFe 2 O 4 /ZnO were prepared by solution combustion method. The characterization of the nano powders was done by powder X-ray diffraction (PXRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM). The ZnO and a-Fe 2 O 3 nanopowders exhibited the wurtzite and hexagonal phases, respectively. The PXRD pattern of ZnFe 2 O 4 /ZnO indicated the spinel phase of zinc ferrite and wurtzite phase of zinc oxide. The threedoi:10.1007/s13204-014-0395-1 fatcat:dicifgo7jrbs3d5mybxh7tiedm