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Department of Chemistry, University of Rajasthan, Jaipur-302 004, Rajasthan, India E-mail : Manuscript received 23 August 2012, revised 30 April 2014, accepted 21 June 2014 Reaction of VO(OPri )3 with HOCMe2 (CH2 )CMe2OH in 1 : 2 molar ratio affords dimeric homometallic glycolate complex, [VO(OGO)(OGOH)]2 (1) (where OGO = doubly deprotonated form of the 2,5-dimethyl-2,5-hexanediol). Reactions of (1) with different metal isoproposides in 1 : 2 molar ratio yield a novel class of heterobimetallicdoi:10.5281/zenodo.5735158 fatcat:ztuss6l3y5g7vno7a5lt735xei