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An electron diffraction investigation of unstable gaseous disulfane using the sector-microphotometer method has been carried out. The results of these measurements and the available microwave data together yield the following molecular parameters for Hd (S—H) = 1.352 ± 0.015 A, angle (HSS) = 91°57′, d(S—S) = 2.055 ± 0.001 A, dihedral angle = 90°37′ ± 3′.doi:10.1515/zna-1968-0109 fatcat:4qxbedfd2nfg5kjhymdi76seui