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Macro/meso/microporous carbon monoliths doped with sulfur have been prepared from sulfonated poly(divinylbenzene) networks followed by the activation with CO 2 resulted in the activated carbon monoliths with high surface area of 2400 m 2 g 1 . The monolithic electrode of the activated carbon shows remarkably high specific capacitance (175 F g 1 at 5 mV s 1 and 206 F g 1 at 0.5 A g 1 ). Increasing demands for the electrochemical devices, such as batteries, 1 fuel cells, 2 and electricdoi:10.1039/c0jm03793a fatcat:s7ep5j7pyzbsfdg622s65y4cbq