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Bulgarian Chemical Communications
Liquid-phase synthesis of N,N'-diacetyl-β-chitobiosyl allosamizoline 2 was studied. The N-benzyloxycarbonyl (Cbz) protected trichloroacetimidate donors 3 and 5 were prepared according to the routine method. The target allosamidin analogue 2 was high-efficiently synthesized by iterative glycosylation reactions, catalytic hydrogenation, acetylation, and deacetylation, respectively.fatcat:37pjrulihzhkpaivtkvhlhybbi