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Materials Dithiobis(succinimidyl propionate) was purchased from Sigma used as supplied. Casein kinase II and peptide (1) were purchased from New England BioLabs. Alkaline phosphatase was purchase from Sigma. Modification of Electrodes with peptide (1) Au wire electrodes (0.5 mm diameter, geometrical area ca. 0.16 cm 2 , roughness factor ca. 1.4) were used in the experiments. Prior to modification, the electrodes were soaked in concentrated HNO 3 for 5 min, rinsed with water. Then the electrodesdoi:10.1039/b800247a pmid:18473075 fatcat:uzx2rg5qgbgi3prjlmqlgbvb2i