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New layered carbon-based materials were prepared and exhaustively characterized exploiting different characterization techniques, such as thermogravimetry (TGA), differential thermal calorimetry (DSC), Fourier transform infrared (FTIR) and wide angle X-ray diffraction (WAXD). Pristine graphite (G) with high surface area and carbon black (CB) samples with different surface areas were selected as starting materials to prepare the corresponding oxidized samples, i.e. graphite oxide (GO) and carbondoi:10.14273/unisa-882 fatcat:7thwjabvyvgsdgdvdd4gpzqbu4