Transition Bimetallic Carbides: Synthesis and Characterization [chapter]

A. I. Reyes, J. A. Melo, J. G. Sandoval, R. Silva Rodrigo, J. M. Dominguez, A. Toledo, D. Acosta
2003 Emerging Fields in Sol-Gel Science and Technology  
Co-Mo carbides were prepared by impregnation with aqueous solution of metal salts and sucrose into ordered mesoporous SBA-15 silica template using carbothermal hydrogen reduction. Bimetallic Co-Mo carbide obtained by using carbothermal hydrogen reduction of Co-Mo precursors is formed when the Co-Mo molar ratio is 1.0. The obtained samples were characterized by X-ray diffraction, scanning electron microscopy and energy dispersive X-ray analysis. Electrochemical characterization of obtained
more » ... n of obtained materials wеre performed by cyclic voltammetry in acid solution.
doi:10.1007/978-1-4615-0449-8_7 fatcat:qtf65nxrdfgxnidlpcdz6g6vmy