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By adopting a simple cost effective microwave-assisted synthesis methodology, nanosized ceria-zirconia solid solution (MW) has been prepared. For comparison purpose, ceria-zirconia solid solution with the same composition was also synthesized by a coprecipitation method (CP) and calcined at 773 K. Both the samples were examined by different characterization techniques namely, X-ray diffraction, Raman spectroscopy, X-ray photoelectron spectroscopy, transmission electron microscopy, BET surfacedoi:10.2174/1874067700903010024 fatcat:qnmii46txfdnde34ioo3ezgkwa