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Synthesis and Characterization of New Copoly(amide-imide)s Based on Bicyclo[2,2,2] oct-7-ene-2,3,5,6-tetracarboxylic diimide and Azobenzene Group in the Main Chain

Khalil Faghihi, Mohsen Hajibeygi, Meisam Shabanian
2009 High Temperature Materials and Processes  

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In this article six new copoly(amide-imide)s CoPAIs 6a-f were synthesized through the direct polycondensation reaction of N,N'-bis(4carboxyphenyl)bicyclo[2,2,2]oct-7-ene-2,3,5,6tetracarboxylic diimide 3 with 4,4'azobenzenedicarboxylic acid 4 in the presence of various diamines 5a-f in a medium consisting of Nmethyl-2-pyrrolidone (NMP), triphenyl phosphite (TPP), calcium chloride (CaQ 2 ) and pyridine (Py). The resulted polymers were fully characterized by means of FTIR spectroscopy, elemental
more » ... alyses, inherent viscosity, solubility tests and UV-vis spectroscopy. Thermal properties of the CoPAIs 6a-f were investigated using thermal gravimetric analysis (TGA and DTG).
doi:10.1515/htmp.2009.28.6.379 fatcat:fkysvzhxdzdldhbyfni5nu4cxm
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Khalil Faghihi, Mohsen Hajibeygi, Meisam Shabanian. "Synthesis and Characterization of New Copoly(amide-imide)s Based on Bicyclo[2,2,2] oct-7-ene-2,3,5,6-tetracarboxylic diimide and Azobenzene Group in the Main Chain." High Temperature Materials and Processes 28.6 (2009)