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The high-temperature gas chromatographic (GC) separation of several semivolatile compounds is studied with a short metal capillary column packed with fibrous material, having a polydimethylsiloxane coating thereon. Taking advantage of the excellent heat-resistance of the fiber and also the combination of the surface-deactivated metal capillary, a temperatureprogrammed separation up to 450°C is successfully demonstrated for the separation of polymer standard samples. The average molecular weightdoi:10.1093/chromsci/43.10.536 pmid:16438796 fatcat:dqdppw7hirbn5kkq5k773ihl4q