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A new organic superconductor β-(meso-DMBEDT-TTF)2PF6
2004
Chemical Communications
General information. The reactions in scheme 1 and electrochemical crystallizations were carried out under a dry nitrogen atmosphere. Triethyl phosphite was distilled under reduced pressure in the presence of sodium and THF was freshly distilled under nitrogen over sodium and benzophenone. Chlorobenzene was washed with conc. H 2 SO 4 then with aq. NaHCO 3 and water, followed by drying with CaCl 2 , and distilled under nitrogen. Melting points were determined with a Yanaco MP micro melting point
doi:10.1039/b409631b
pmid:15514812
fatcat:nexn4ytllrczzplfickd5dd64q