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OXIDATIVE DESULPHURIZATION OF 1-SUBSTITUTED 1Н-TETRAZOLE-5-THIOLES
ОКИСЛИТЕЛЬНОЕ ДЕСУЛЬФИРОВАНИЕ 1-ЗАМЕЩЕННЫХ 1Н-ТЕТРАЗОЛ-5-ТИОЛОВ

Leonid V. Myznikov, St. Petersburg State Institute of Technology (Technical University), Svetlana V. Vorona, Yurii E. Zevatskii, St Petersburg State Institute of Technology (Technical University), St Petersburg State University of Industrial Technologies and Design;St Petersburg State Institute of Technology (Technical University)
2019 Bulletin of the Saint Petersburg State Institute of Technology (Technical University)  

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An effective method for the synthesis of 1-substituted 1H-tetrazoles by oxidative desulphurization of 1-substituted 1H-tetrazole-5-thiols with hydrogen peroxide in acetonitrile in the presence of a catalytic amount of trifluoroacetic acid is proposed. The main advantages of the proposed method are high yields of target products, mild conditions and short reaction time.
doi:10.36807/1998-9849-2019-48-74-9-12 fatcat:pehg3zbgknf3pfrll6qtotf7fi
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Leonid V. Myznikov, St. Petersburg State Institute of Technology (Technical University), Svetlana V. Vorona, Yurii E. Zevatskii, St Petersburg State Institute of Technology (Technical University), St Petersburg State University of Industrial Technologies and Design;St Petersburg State Institute of Technology (Technical University). "OXIDATIVE DESULPHURIZATION OF 1-SUBSTITUTED 1Н-TETRAZOLE-5-THIOLES." Bulletin of the Saint Petersburg State Institute of Technology (Technical University) (2019) 9-12