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The interphase area appears to have a great impact on nanocomposite (NC) dielectric properties. However, the underlying mechanisms are still poorly understood, mainly because the interphase properties remain unknown. This is even more true if the temperature increases. In this study, a multiscale characterization of polyimide/silicon nitride (PI/Si3N4) NC dielectric properties is performed at various temperatures. Using a nanomechanical characterization approach, the interphase width wasdoi:10.3390/polym13121936 fatcat:dwxn4ejtmnfpdkenzxihju3m3u