A copy of this work was available on the public web and has been preserved in the Wayback Machine. The capture dates from 2017; you can also visit the original URL.
The file type is application/pdf
.
Structure Determination for the Crystalline Phase of Triphenyl Phosphite by Means of Multi-Dimensional Solid-State NMR and X-Ray Diffraction
2001
Zeitschrift für Naturforschung. B, A journal of chemical sciences
The crystalline phase of triphenyl phosphite P(OC6H5)3 was investigated by means of 31P solid-state NMR and X-ray diffraction in a temperature range between 170 K and its melting point (Tm = 293 K). ID MAS NMR spectra exhibit one sharp central resonance indicating only one crystallographically unique molecule in the unit cell. A theoretical analysis concerning the shape of 2D exchange spectra for 1 = 1 /2 nuclei is presented. It is shown that if the exchange is caused by radio-frequency driven
doi:10.1515/znb-2001-1101
fatcat:slidkuob6vd4ddpmzusjmuxb3i