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Three-electrode measurements are valuable to the understanding of the electrochemical processes in a battery system. However, their application in lithium–sulfur chemistry is difficult due to the complexity of the system and thus rarely reported. Here, we present a simple three-electrode cell format with relatively good life time and minimum interference with the cell operation.doi:10.26434/chemrxiv-2021-gznvz fatcat:6umsdzznnzfvzgpchycygxt3ue