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In this work we report the synthesis and characterization of hybrid nanostructures of multiwall carbon nanotubes (MWCNT) and cadmium sulphide (CdS) nanoparticles. In a solution of thioacetamide and cadmium sulphide, purified MWCNT are added to prepare the CNT/CdS hetrostructure. XRD diagrams, SEM images, and also photoluminescence spectra of the prepared samples are analyzed. SEM images show the CdS nanoparticles of 17nm size coated on the CNTs. Visible photoluminescence with peaks at 435 nmdoaj:e6d240ad7bd549e2849b41b23590f49d fatcat:4wdlnbst7zfutciyrx72fbtgui