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Large Telluroxane Bowls Connected by a Layer of Iodine Ions
2021
Angewandte Chemie
Phenyltelluroxane clusters of the composition [{(PhTe) 19 O 24 } 2 I 18 (solv)] (1)a re formed during the hydrolysis of [PhTeI 3 ] 2 or the oxidation of various phenyltellurium(II) compounds with iodine under hydrolytic conditions.T he compounds consist of two half-spheres with a{(PhTe) 19 O 24 } 9+ network, which are connected by 18 iodine atoms.T he spherical clusters can accommodate solvent molecules such as pyridine or methanol in the center of two rings formed by iodine atoms.T he presence
doi:10.1002/ange.202103700
fatcat:gzmrlc4bcffhnbxypfarv7g2jy